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          Applications of Synchrotron Radiation for Environmental Sciences and Materials Research for Development of Environmentally Friendly Resources

          Closed for proposals

          Project Type

          Coordinated Research Project

          Project Code

          F11015

          CRP

          1751

          Approved Date

          15 July 2011

          Status

          Closed

          Start Date

          10 February 2012

          Expected End Date

          9 February 2016

          Completed Date

          18 February 2016

          Description

          Synchrotron radiation (SR) laboratories offer a wide variety of techniques that can be applied to the study of matter. The scientists making use of Synchrotron radiation come from many different fields ranging from physics and chemistry, to materials, environmental and life sciences. Synchrotron science is advancing rapidly.? This includes the development of ‘4th-generation’ sources, significant upgrades to storage ring based sources and advances in optics and detectors. Remote access mechanisms are being established by most facilities, providing additional access opportunities.? Facilities and users in developing countries could also benefit from these developments and many countries have already taken action in this direction. Since the SR facility can be used in many fields, it can foster inter-disciplinary research activities within as well as between countries. One of the fast growing applications of SR is in environmental science and engineering, and it would be appropriate and relevant to the IAEA mandates and needs of Member States, to formulate a CRP on application of SR focussing on two important areas, namely Materials and Environmental Sciences. This project is expected to build capabilities to use SR, to develop research programs in this area and finally lead to socio-economic development in the MS.

          Objectives

          Optimization of Synchrotron X-ray Radiation based techniques for applications in Material sciences and environmental sciences.

          Specific objectives

          Study the role of the crystallisation enhancer in building ceramics (conventional brick, earthenware or industrial ceramics, where the role of metal containing crystallisation enhancers is often determined empirically) using SR based techniques

          Establishment of interdisciplinary research programs based on the use of SR for the development of new mining technologies that are environmentally sustainable.

          Application of SR to optimize the preparation of conventional building materials such as cements and concrete

          Establishment of synchrotron measurements, particularly XAS, as new and reliable tools for environmental monitoring.

          Establishment of comprehensive interdisciplinary research programs based on the use of SR, that can span a complete range of processes including analysis of solid mine tailings, that have an implication on the food chain.

          Impact

          The CRP utilized SR and complimentary methodologies including ion beam analysis to provide improved characterization and better understanding of materials properties, and their interactions of environmental relevance, such as chemical speciation of a variety of elements in a wide spatial range. With this new information, advances in the following fields were obtained: Advanced understanding of metal bioavailability and its impact on the establishment of vegetation in contaminated sites; Increased awareness about potential toxic effects among population and governmental official sectors; Appraisal of human health hazards by toxic elements contained in agricultural products; Preventive conservation of artworks by increasing awareness of photo aging process and recommending to museum curators appropriate preventing measures such as lowering of ambient light levels for some paintings and more systematic use of transparent covers (glass covers or intact varnish layers).

          CRP Publications

          Type

          article

          Year

          2015

          Description

          Morales-López Gladys, de la Rosa-álvarez Ma. Guadalupe, García-Jiménez Ma. Guadalupe, Delgado-Ríos Marcos, Rocha-Amador Diana O., Castillo-Michel Hiram, Gardea-Torresdey Jorge, Cruz-Jiménez Gustavo. Iron speciation in PM10 from a Mexican city: X-ray absorption spectroscopy as a tool for the identification of the potential source of pollution. Prepared for Environmental Geochemistry

          Country/Organization

          Mexico/ Universidad de Guanajuato

          Type

          article

          Year

          2015

          Description

          M. Harfouche, G. Aquilanti, A. M. Ghrair, D. M. Jaradat and A. AlDarabee (2015) Elemental distribution and structural behavior of heavy metals in Jordan soils: an XRF and XAFS study (in preparation)

          Country/Organization

          Jordan/SESAME

          Type

          Original Article

          Year

          2014

          Publication URL

          https://doi.org/10.1080/15226514.2013.810584

          Description

          Authors: Guadalupe de la Rosa, Hiram Castillo-Michel, Gustavo Cruz-Jiménez, Jesús Bernal-Alvarado, Teodoro Córdova-Fraga, Laura López-Moreno and Marine Cotte; Paper title: Cr Localization and Speciation in Roots of Chromate Fed Helianthus annuus L. Seedlings Using Synchrotron Techniques; Journal: International Journal of Phytoremediation, Vol. 16, Pages 1073-1086, Year 2014

          Country/Organization

          MEXICO (Univ. of Guanajuato), FRANCE (ESRF Grenoble), PUERTO RICO (Univ. of Puerto Rico)

          Type

          Original Article

          Year

          2013

          Publication URL

          https://doi.org/10.1111/pce.12234

          Description

          Authors: Isabelle Lefèvre, Katarina Vogel-Miku?, Luka Jeromel, Primo? Vavpetic, Sébastien Planchon, Iztok Arcon, Johannes T. Van Elteren, Gilles Lepoint, Sylvie Gobert, Jenny Renaut, Primo? Pelicon, Stanley Lutts; Paper title: Differential cadmium and zinc distribution in relation to their physiological impact in the leaves of the accumulating Zygophyllum fabago L., Journal: Plant, Cell and Environment, Vol. 37, Pages 1299–1320, Year 2014

          Country/Organization

          BELGIUM (Université catholique de Louvain and University of Liège), SLOVENIA (Univ. of Ljubljana, Jo?ef Stefan Inst., Univ. of Nova Gorica and Nat. Inst. of Chemistry), LUXEMBOURG (Centre de Recherche Public, Belvaux)

          Type

          article

          Year

          2013

          Description

          SINGH, Sudhir P., VOGEL-MIKU?, Katarina, VAVPETIC, Primo?, JEROMEL, Luka, PELICON, Primo?, KUMAR, Jitendra, TULI, Rakesh. Spatial X-ray fluorescence micro-imaging of minerals in grain tissues of wheat and related genotypes. Planta, 2014, 277-289, doi: 10.1007/s00425-014-2084-4

          Country/Organization

          Slovenia/ University of Ljubljana

          Type

          Journal Article

          Year

          2015

          Publication URL

          https://www.jstor.org/stable/24921502

          Description

          Authors: René Loredo Portales, Gustavo Cruz Jiménez, Hiram Castillo Michel, Diana Olivia Rocha Amador, Katarina Vogel Miku?, Peter Kump and Guadalupe de la Rosa; Paper title: Understanding Copper speciation and mobilization in soils and mine tailings from “Mineral La Aurora” in central Mexico; Journal: Boletín de la Sociedad Geológica Mexicana, Vol. 67, Pages 447-456, Year 2015

          Country/Organization

          MEXICO (Univ. of Guanajuato), FRANCE (ESRF Grenoble), SLOVENIA (Univ. of Ljubljana and Jo?ef Stefan Institute)

          Type

          Research Paper

          Year

          2014

          Publication URL

          https://doi.org/10.1016/j.jphotobiol.2013.10.011

          Description

          Authors: Katja Klancnik, Katarina Vogel-Miku?, Alenka Gaber?cik; Paper title: Silicified structures affect leaf optical properties in grasses and sedge; Journal: Journal of Photochemistry and Photobiology B: Biology Vol. 130, Pages 1-10, Year 2014

          Country/Organization

          SLOVENIA (University of Ljubljana)

          Type

          article

          Year

          2013

          Description

          Guadalupe de la Rosa, Hiram Castillo-Michel, Gustavo Cruz-Jiménez, Jesús Bernal-Alvarado, Teodoro Córdova-Fraga, Laura López-Moreno, Marine Cotte. "Cr localization and speciation in roots of chromate fed Helianthus annuus L. seedlings using synchrotron techniques" 2013. International Journal of Phytoremediation. DOI: 10.1080/15226514.2013.810584.

          Country/Organization

          Mexico/ Universidad de Guanajuato

          Type

          article

          Year

          2014

          Description

          Dinámica de Arsénico en el Sistema de Jales Mineros de ¨La Aurora¨: Importancia de la Interdisciplinariedad en la resolución de Problemas Ambientales. Guadalupe de la Rosa, J. Jesús Ibarra Sánchez, Gustavo Cruz-Jiménez, Rene Loredo-Portales, Katarina Vogel, Hiram Castillo-Michel. Proceedings XXXV Encuentro Nacional de la AMIDIQ. 759-763. 2014. ISBN 978-607-95593-2-8.

          Country/Organization

          Mexico/ Universidad de Guanajuato

          Type

          article

          Year

          2012

          Description

          Tserenpil Sh., Liu C-Q., Wang L. 2012. Antimony binding to soil-derived humic acid: Nuclear Magnatic Resonance and X-Ray Absorption Fine Structure Spectroscopy study. Microchemical journal. 68-73.

          Country/Organization

          Mongolia/ National University of Mongolia

          Type

          article

          Year

          2015

          Description

          Messaoud Harfouche, Ayoup M. Ghrair, Da’san M. Jaradat, Riyad M. Jaber, Nashat Swai and Giuliana Aquilanti (2015) Absorption and Mobility of Cr and Zn in Soil in the Vicinity of Jordan River XAFS16 conference, Karlsruhe Germany, August 2015(will be published in the conference proceedings)

          Country/Organization

          Jordan/SESAME

          Type

          Research Paper

          Year

          2017

          Publication URL

          https://doi.org/10.1016/j.jece.2017.01.019

          Description

          Authors: R. Loredo-Portales, H. Castillo-Michel, G. Aquilanti, Ma. G. De La Rosa-álvarez, D. O. Rocha-Amador, K. Vogel-Mikus, P. Kump, G. Cruz-Jiménez; Paper title: Synchrotron based study of As mobility and speciation in tailings from a mining site in Mexico; Journal: Journal of Environmental Chemical Engineering, Vol. 5, Pages 1140-1149, Year 2017

          Country/Organization

          MEXICO (Univ. of Guanajuato), FRANCE (ESRF Grenoble), ITALY (Elettra-Sincrotrone), SLOVENIA (Univ. of Ljubljana and Jo?ef Stefan Institute)

          Type

          article

          Year

          2015

          Description

          René Loredo Portales, Gustavo Cruz Jiménez, Hiram Castillo Michel, Diana Olivia Rocha Amador, Katarina Vogel Mikus, Peter Kump, Guadalupe de la Rosa. Arsenic speciation and mobility in mine tailings from the Guanajuato mining District. In preparation.

          Country/Organization

          Mexico/ Universidad de Guanajuato

          Type

          article

          Year

          2014

          Description

          LEFEVRE, Isabelle, VOGEL-MIKU?, Katarina, JEROMEL, Luka, VAVPETIC, Primo?, PLANCHON, Sébastien, ARCON, Iztok, ELTEREN, Johannes Teun van, LEPOINT, Gilles, GOBERT, Sylvie, RENAUT, Jenny, PELICON, Primo?, LUTTS, Stanley. Differential cadmium and zinc distribution in relation to their physiological impact in the leaves of the accumulating Zygophyllum fabago L. Plant, cell and environment, 2014, 1299-1320, doi: 10.1111/pce.12234

          Country/Organization

          Slovenia/ University of Ljubljana

          Type

          article

          Year

          2014

          Description

          KLANCNIK, Katja, VOGEL-MIKU?, Katarina, GABER?CIK, Alenka. Silicified structures affect leaf optical properties in grasses and sedge. Journal of photochemistry and photobiology. B, Biology, 2014, 1-10. doi: 10.1016/j.jphotobiol.2013.10.011

          Country/Organization

          Slovenia/ University of Ljubljana

          Type

          Book Chapter

          Year

          2012

          Publication URL

          https://doi.org/10.1201/b12954

          Description

          Authors: Katarina Vogel-Miku?, Iztok Arcon, Peter Kump, Primo? Pelicon, Marijan Necemer, Primo? Vavpetic, Marjana ?pela; Title: (Chapter 25) Analytical tools for exploring metal accumulation and tolerance in plants; Journal: Book “Phytotechnologies”, edited by Naser A. Anjum, Maria E. Pereira, Iqbal Ahmad, Armando C. Duarte, Shahid Umar, and Nafees A. Khan (CRC Press, Boca Raton, 2012), pages 443 - 496

          Country/Organization

          SLOVENIA (Univ. of Ljubljana, Jo?ef Stefan Institute and Univ. of Nova Gorica)

          Type

          article

          Year

          2013

          Description

          VOGEL-MIKU?, Katarina, ARCON, Iztok, KUMP, Peter, PELICON, Primo?, NECEMER, Marijan, VAVPETIC, Primo?, KOREN, ?pela, REGVAR, Marjana. Analytical tools for exploring metal accumulation and tolerance in plants. V: ANJUM, Naser A. (ur.). Phytotechnologies: remediation of environmental contaminants. Boca Raton (FL): Taylor & Francis, cop. 2013, 443-495.

          Country/Organization

          Slovenia/ University of Ljubljana

          Type

          article

          Year

          2015

          Description

          Xibai Zeng , Shiming Su, Qiufen Feng, Xiurong Wang, Yangzhu Zhang, Lili Zhang, Sheng Jiang, Aiguo Li, Lianfang Li, Yanan Wang, Cuixia Wu, Lingyu Bai, Ran Duan, Arsenic speciation transformation and arsenite influx and efflux across the cell membrane of fungi investigated using HPLC–HG–AFS and in-situ XANES, Chemosphere 119 (2015) 1163–1168

          Country/Organization

          China/Institute of Environment and Sustainable Development in Agriculture, Chinese Academy of Agricultural Sciences

          Type

          Article

          Year

          2013

          Publication URL

          https://link.springer.com/article/10.1007/s11104-013-1617-0

          Description

          Authors: ?pela Koren, Iztok Arcon, Peter Kump, Marijan Necemer and Katarina Vogel-Miku?; Paper title: Influence of CdCl2 and CdSO4 supplementation on Cd distribution and ligand environment in leaves of the Cd hyperaccumulator Noccaea (Thlaspi) praecox; Journal: Plant Soil, Vol. 370, pages 125–148, Year 2013

          Country/Organization

          SLOVENIA (University of Ljubljana, University of Nova Gorica, and Jo?ef Stefan Institute)

          Type

          Paper

          Year

          2015

          Publication URL

          https://doi.org/10.1039/C4EM00603H

          Description

          Authors: Lisa L. Van Loon, Cassidy Throssell and Michael D. Dutton; Paper title: Comparison of nickel speciation in workplace aerosol samples using sequential extraction analysis and X-ray absorption near-edge structure spectroscopy; Journal: Environmental Science: Processes & Impacts, Vol. 17, Pages 922-931, Year 2015

          Country/Organization

          CANADA (Canadian Light Source Inc., Saskatoon, SK, Canada)

          Type

          Conference Proceedings Paper

          Year

          2014

          Publication URL

          https://www.dropbox.com/s/oe4d8luw4ndck2x/2014.pdf

          Description

          Authors: Guadalupe de la Rosa, J. Jesús Ibarra Sánchez, Gustavo Cruz-Jiménez, Rene Loredo-Portales, Katarina Vogel, Hiram Castillo-Michel; Paper title: Dinámica de Arsénico en el Sistema de Jales Mineros de ¨La Aurora¨: Importancia de la Interdisciplinariedad en la resolución de Problemas Ambientales; Journal: Memorias del XXXV Encuentro Nacional de la AMIDIQ (Puerto Vallarta, México, May 6-9, 2014), published by Academia Mexicana de Investigación y Docencia en Ingeniería Química (AMIDIQ); Pages 759-763, Year 2014 ISBN 978-607-95593-2-8

          Country/Organization

          MEXICO (Univ. of Guanajuato), FRANCE (ESRF Grenoble), SLOVENIA (Univ. of Ljubljana and Jo?ef Stefan Institute)

          Type

          article

          Year

          2013

          Description

          SINGH, Sudhir P., VOGEL-MIKU?, Katarina, ARCON, Iztok, VAVPETIC, Primo?, JEROMEL, Luka, PELICON, Primo?, KUMAR, Jitendra, TULI, Rakesh. Pattern of iron distribution in maternal and filial tissues in wheat grains with contrasting levels of iron. Journal of Experimental Botany, 2013, 3249-3260, doi: 10.1093/jxb/ert160.

          Country/Organization

          Slovenia/ University of Ljubljana

          Type

          article

          Year

          2015

          Description

          Tserenpil Sh., Sapkota A., Peng J-H., Liu C-Q, Liu B. 2015. Variation in lead isotopic ratios in Mongolian urban and rural soils. Euroasian Soil Sciences (under review).

          Country/Organization

          Mongolia/ National University of Mongolia

          Type

          article

          Year

          2013

          Description

          KOREN, ?pela, ARCON, Iztok, KUMP, Peter, NECEMER, Marijan, VOGEL-MIKU?, Katarina. Influence of CdCl2 and CdSO4 supplementation on Cd distribution and ligand environment in leaves of the Cd hyperaccumulator Noccaea (Thlaspi) praecox. Plant and soil, 2013, 125-148, doi: 10.1007/s11104-013-1617-0.

          Country/Organization

          Slovenia/ University of Ljubljana

          Type

          article

          Year

          2015

          Description

          René Loredo Portales, Gustavo Cruz Jiménez, Hiram Castillo Michel, Diana Olivia Rocha Amador, Katarina Vogel Mikus, Peter Kump, Guadalupe de la Rosa. “Understanding Copper speciation and mobilization in soils and mine tailings from “Mineral La Aurora” in central Mexico: contributions from Synchrotron techniques“. 2015. Boletín de la Sociedad Geológica de México. Accepted

          Country/Organization

          Mexico/ Universidad de Guanajuato

          Type

          Doctoral thesis

          Year

          2013

          Description

          KOREN, ?pela. Vpliv kadmija na mineralno prehrano in metabolizem ogljikovih hidratov pri ranem mo?njaku (Thlaspi praecox Wulf.): doktorska disertacija = Impact of cadmium on mineral nutrition and carbohydrate metabolism in pennycress (Thlaspi praecox Wulf.): doctoral dissertation. Ljubljana: [?. Koren], 2013. 133 p. (supervisor prof.dr. Marjana Regvar, co-supervisor prof.dr. Katarina Vogel-Miku?)

          Country/Organization

          Slovenia/ University of Ljubljana

          Type

          Doctoral Dissertation

          Year

          2013

          Publication URL

          https://repozitorij.uni-lj.si/Dokument.php?id=138680

          Description

          Authors: ?pela Koren; Title: Impact of cadmium on mineral nutrition and carbohydrate metabolism in pennycress (Thlaspi praecox Wulf.) [Vpliv kadmija na mineralno prehrano in metabolizem ogljikovih hidratov pri ranem mo?njaku (Thlaspi praecox Wulf.)]; Supervised by Prof. Alenka GABER?CIK, Dr. Katarina VOGEL-MIKU?, Prof. Marjana REGVAR and Dr. Primo? PELICON

          Country/Organization

          SLOVENIA (Univ. of Ljubljana and Jo?ef Stefan Institute)

          Type

          Original Article

          Year

          2014

          Publication URL

          https://link.springer.com/article/10.1007/s00425-014-2084-4

          Description

          Authors: Sudhir P. Singh, Katarina Vogel-Miku?, Primo? Vavpetic, Luka Jeromel, Primo? Pelicon, Jitendra Kumar, and Rakesh Tuli; Paper title: Spatial X-ray fluorescence micro-imaging of minerals in grain tissues of wheat and related genotypes; Journal: Planta, Vol. 240, pages 277–289, Year 2014

          Country/Organization

          INDIA (Nat. Agri-Food Biotechnology Institute, Mohali 160071), and SLOVENIA (University of Ljubljana and Jo?ef Stefan Institute)

          Type

          Research Paper

          Year

          2013

          Publication URL

          https://doi.org/10.1093/jxb/ert160

          Description

          Authors: Sudhir P. Singh, Katarina Vogel-Miku?, Iztok Arcon, Primo? Vavpetic, Luka Jeromel, Primo? Pelicon, Jitendra Kumar, and Rakesh Tuli; Paper title: Pattern of iron distribution in maternal and filial tissues in wheat grains with contrasting levels of iron; Journal: Journal of Experimental Botany, Vol. 64, pages 3249–3260, Year 2013

          Country/Organization

          INDIA (Nat. Agri-Food Biotechnology Institute, Mohali 160071), and SLOVENIA (University of Ljubljana, University of Nova Gorica, and Jo?ef Stefan Institute)

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